| 10th October 2020 04:30 PM | |
| KunwarR | Sathyabama Institute of Science and Technology B.E. - Electronics and Instrumentation Engineering SEIA1502 Analytical Instrumentation Syllabus Sathyabama Institute of Science and Technology B.E. - Electronics and Instrumentation Engineering SEIA1502 Analytical Instrumentation Syllabus SATHYABAMA INSTITUTE OF SCIENCE AND TECHNOLOGY SEIA1502 ANALYTICAL INSTRUMENTATION UNIT 1 SPECTRO PHOTOMETERS 9 Hrs. Spectral methods of analysis – Beer’s law UV – visible spectrophotometers – single beam and double beam instruments – source and detectors – IR spectrophotometers – sources and detectors – FTIR spectrometers –Atomic absorption spectrophotometer – flame emission spectrophotometers – sources of flame photometry –applications - ESR, EPR spectroscopy - TOF spectrometer -Introduction to x-ray spectroscopy. UNIT 2 PRINCIPLE of NUCLEAR MAGNETIC RESONANCE 9 Hrs. NMR – basic principle – NMR spectrometers – applications – introduction to mass spectrophotometers –nuclear radiation detectors – GM counter – proportional counter – solid state detectors. UNIT 3 CHROMATOGRAPHY 9 Hrs. Gas chromatography – liquid chromatography –– high-pressure liquid chromatography – principles, types and applications detectors. UNIT 4 pH CONDUCTIVITY & DISSOLVED COMPONENT ANALYSER 9 Hrs. Conductivity meters – pH meters - dissolved oxygen hydrogen analyser –sodium analyser – silica analyser and Sampling systems. UNIT 5 GAS ANALYSER 9 Hrs. Thermal conductivity - thermal analyser – types of Oxygen analyser – CO monitor – NOx analyser – H2S analyser – dust and smoke measurement Max. 45 Hrs. COURSE OUTCOMES On completion of the course, student will be able to CO1 - Understand the working of different types of Analysers. CO2 - Analyze the techniques of chromatography. CO3 - Understand working of different Spectrophotometers. CO4 - Explain NMR. CO5 - Analyze the applications of Analyzers, Chromatography. CO6 - Explain the operating principle of analyzers, chromatography, Spectrophotometers. TEXT/ REFERENCE BOOKS 1. Hobart H. Willard, Lynne.L. Merrit, John A. Dean, Frank A.Settle, “Instrumental Methods of Analysis”, 7th Edition, CBS Publishing & Distribution, 1986. 2. Jain R.K, “Mechanical &Industrial Measurements”, Khanna Publishers, 11th Edition, 2004. 3. Khandpur R.S, “Handbook of Analytical Instruments”, II Edition, Tata McGrawHill, New Delhi, 2006. 4. Gurdeep R. Chatwal, Sham.K. Anand, “Instrumental methods of Chemical Analysis” Himalaya Publishing house, Reprint 2006. 5. Robert D. Braun, “Introduction to Instrumental Analysis”, Pharma Book Syndicate, Hyderabad, Reprint 2006. 6. Douglas.A. Skoog, F.James Holker, Stanley R.Gouch, “Instrumental Analysis”, Engage Learning India, India Edn.2008. END SEMESTER EXAM QUESTION PAPER PATTERN Max. Marks: 100 Exam Duration: 3 Hrs. PART A: 10 Questions of 2 marks each-No choice 20 Marks PART B: 2 Questions from each unit of internal choice, each carrying 16 marks 80 Marks |
