| 27th October 2020 09:32 AM | |
| KunwarR | Sathyabama Institute of Science and Technology B.Sc - Chemistry SCY4111 Inorganic quantitative analysis and preparations Syllabus Sathyabama Institute of Science and Technology B.Sc - Chemistry SCY4111 Inorganic quantitative analysis and preparations Syllabus SATHYABAMA INSTITUTE OF SCIENCE AND TECHNOLOGY DEPT. OF CHEMISTRY SCY 4111 INORGANIC QUANTITATIVE ANALYSIS AND PREPARATIONS L T P Credits Total Marks 0 0 3 2 100 VOLUMETRIC ANALYSIS: 1. Acid – base titrations: a. Estimation of HCl. b. Estimation of oxalic acid. 2. Redox titrations: a. Estimation of Ferrous ammonium sulphates (Permanganometry). b. Estimation of KMnO4 (Iodometry). c. Estimation of Copper (Iodometry). 3. Complexometric titration: a. Estimation of calcium using EDTA. INORGANIC PREPARATIONS a. Preparation of Ferrous ammonium sulphate. b. Preparation of tetraammine copper(II) sulphate. c. Preparation of potassium trioxalatoaluminate. d. Preparation of potassium trioxalatochromate COURSE OUTCOMES On successful completion of the course, student will be able to CO1:Estimate the amount of analyte by acid-base titration. CO2  etermine the amount of analyte by Redox titration.CO3:Estimate the amount of calcium by complexometric titration. CO4:Prepare crystals of Mohr's salt. CO5:Synthesize crystals of copper salt CO6:Prepare crystals of oxalato complexes of aluminum and chromium. TEXT / REFERENCE BOOKS 1). S. Sundaram and K. Raghavan, Practical Chemistry, S. Viswanathan Co. Pvt., 1996. 2). N. S. Ganapragasam and G. Ramamurthy, Organic Chemistry – Lab manual, S.Viswanathan Co. Pvt., 2002. 3. B.S. Furniss, A.J. Hannaford, P.W. G. Smith and A.R. Tatchell, Vogel’s Text Book of Practical Organic Chemistry.5th ed., Pearson Education, 2005. END SEMESTER EXAM QUESTION PAPER PATTERN Max. Marks: 50 Exam Duration: 2 Hrs. CAE Evaluation of Regular Lab class 15 Marks 25 Marks Model practical exam 10 Marks ESE End Semester Practical exam 25 Marks |
