Sathyabama Institute of Science and Technology B.E. - Electronics and Instrumentation Engineering SEIA1502 Analytical Instrumentation Syllabus

[KunwarR]

Sathyabama Institute of Science and Technology B.E. - Electronics and Instrumentation Engineering SEIA1502 Analytical Instrumentation Syllabus

SATHYABAMA INSTITUTE OF SCIENCE AND TECHNOLOGY

SEIA1502 ANALYTICAL INSTRUMENTATION

UNIT 1 SPECTRO PHOTOMETERS 9 Hrs.
Spectral methods of analysis – Beer’s law UV – visible spectrophotometers – single beam and double beam instruments –
source and detectors – IR spectrophotometers – sources and detectors – FTIR spectrometers –Atomic absorption
spectrophotometer – flame emission spectrophotometers – sources of flame photometry –applications - ESR, EPR
spectroscopy - TOF spectrometer -Introduction to x-ray spectroscopy.

UNIT 2 PRINCIPLE of NUCLEAR MAGNETIC RESONANCE 9 Hrs.
NMR – basic principle – NMR spectrometers – applications – introduction to mass spectrophotometers –nuclear radiation
detectors – GM counter – proportional counter – solid state detectors.

UNIT 3 CHROMATOGRAPHY 9 Hrs.
Gas chromatography – liquid chromatography –– high-pressure liquid chromatography – principles, types and applications
detectors.

UNIT 4 pH CONDUCTIVITY & DISSOLVED COMPONENT ANALYSER 9 Hrs.
Conductivity meters – pH meters - dissolved oxygen hydrogen analyser –sodium analyser – silica analyser and Sampling
systems.

UNIT 5 GAS ANALYSER 9 Hrs.
Thermal conductivity - thermal analyser – types of Oxygen analyser – CO monitor – NOx analyser – H2S analyser – dust
and smoke measurement
Max. 45 Hrs.

COURSE OUTCOMES
On completion of the course, student will be able to
CO1 - Understand the working of different types of Analysers.
CO2 - Analyze the techniques of chromatography.
CO3 - Understand working of different Spectrophotometers.
CO4 - Explain NMR.
CO5 - Analyze the applications of Analyzers, Chromatography.
CO6 - Explain the operating principle of analyzers, chromatography, Spectrophotometers.

TEXT/ REFERENCE BOOKS
1. Hobart H. Willard, Lynne.L. Merrit, John A. Dean, Frank A.Settle, “Instrumental Methods of Analysis”, 7th Edition, CBS
Publishing & Distribution, 1986.
2. Jain R.K, “Mechanical &Industrial Measurements”, Khanna Publishers, 11th Edition, 2004.
3. Khandpur R.S, “Handbook of Analytical Instruments”, II Edition, Tata McGrawHill, New Delhi, 2006.
4. Gurdeep R. Chatwal, Sham.K. Anand, “Instrumental methods of Chemical Analysis” Himalaya Publishing house,
Reprint 2006.
5. Robert D. Braun, “Introduction to Instrumental Analysis”, Pharma Book Syndicate, Hyderabad, Reprint 2006.
6. Douglas.A. Skoog, F.James Holker, Stanley R.Gouch, “Instrumental Analysis”, Engage Learning India, India Edn.2008.


END SEMESTER EXAM QUESTION PAPER PATTERN
Max. Marks: 100 Exam Duration: 3 Hrs.
PART A: 10 Questions of 2 marks each-No choice 20 Marks
PART B: 2 Questions from each unit of internal choice, each carrying 16 marks 80 Marks