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Default Sathyabama Institute of Science and Technology B.Sc - Chemistry SCY4111 Inorganic quantitative analysis and preparations Syllabus

Sathyabama Institute of Science and Technology B.Sc - Chemistry SCY4111 Inorganic quantitative analysis and preparations Syllabus


SATHYABAMA INSTITUTE OF SCIENCE AND TECHNOLOGY DEPT. OF CHEMISTRY

SCY 4111 INORGANIC QUANTITATIVE ANALYSIS AND PREPARATIONS
L T P Credits Total Marks
0 0 3 2 100

VOLUMETRIC ANALYSIS:
1. Acid – base titrations:
a. Estimation of HCl.
b. Estimation of oxalic acid.
2. Redox titrations:
a. Estimation of Ferrous ammonium sulphates (Permanganometry).
b. Estimation of KMnO4 (Iodometry).
c. Estimation of Copper (Iodometry).
3. Complexometric titration:
a. Estimation of calcium using EDTA.


INORGANIC PREPARATIONS
a. Preparation of Ferrous ammonium sulphate.
b. Preparation of tetraammine copper(II) sulphate.
c. Preparation of potassium trioxalatoaluminate.
d. Preparation of potassium trioxalatochromate

COURSE OUTCOMES
On successful completion of the course, student will be able to
CO1:Estimate the amount of analyte by acid-base titration.
CO2etermine the amount of analyte by Redox titration.
CO3:Estimate the amount of calcium by complexometric titration.
CO4:Prepare crystals of Mohr's salt.
CO5:Synthesize crystals of copper salt
CO6:Prepare crystals of oxalato complexes of aluminum and chromium.

TEXT / REFERENCE BOOKS
1). S. Sundaram and K. Raghavan, Practical Chemistry, S. Viswanathan Co. Pvt., 1996.
2). N. S. Ganapragasam and G. Ramamurthy, Organic Chemistry – Lab manual, S.Viswanathan Co. Pvt., 2002.
3. B.S. Furniss, A.J. Hannaford, P.W. G. Smith and A.R. Tatchell, Vogel’s Text Book of Practical Organic Chemistry.5th ed., Pearson Education, 2005.

END SEMESTER EXAM QUESTION PAPER PATTERN
Max. Marks: 50 Exam Duration: 2 Hrs.
CAE Evaluation of Regular Lab class 15 Marks
25 Marks
Model practical exam 10 Marks
ESE End Semester Practical exam 25 Marks
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